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Das Produkt wurde isoliert durch wiederholte Zentrifugation bei 3500 rpm, wobei das Produkt vorgngig in einem Gemisch von 100 ml Ethanol und 50 ml Diethylether und anschliessend in reinem Diethylether suspendiert wurde.To a solution of 4.05 g of the compound of formula 3a in 55 ml of dry DMSO, stirred at room temperature under argon, a solution of 2.60 g of (L) -lysine (2 equivalents) in 15 ml of DMSO was added dropwise

Zou J, Huang R, Li H, Wang B, Chen Y, Chen S, Ou K, Wang X